38MbAbstractThe Xiphos is a new diffractometer that has been been designed and built to determine the solid state structures of materials at ultra low temperatures. As one of very few single crystal X ray diffractometers capable of collecting diffraction data from crystals cooled to 2 K, the Xiphos has an enormous potential for improving our understanding of the relationship between the solid state structure and the physical properties of many materials which show interesting and valuable behaviour at ultra low temperatures. However, there are some challenges to collecting good quality data due to the beryllium vacuum shrouds surrounding the crystal which are necessary components of the cryostat used for reaching these low temperatures.
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